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5. Synthesis and Characterization of Ferrocenyl Substituted Styryl Octasilsesquioxane

Synthesis and Characterization of Ferrocenyl Substituted Styryl Octasilsesquioxane

来源 :中国化学快报（英文版） | 被引量 : 0次 | 上传用户：lzxs123

【摘 要】

：

4-(2-Ferrocenylethenyl)-phenyl-POSS Fc-CH=CH-C6H6-(C5H9)7Si8O12 (FEPS, Fc:ferrocene), containing metal and C=C double bond, was firstly synthesized as a mixture

【作 者】

：

Xiao Yan SONG Hai Ping GENG Qi 

【机 构】

：

College of material science and engineering

【出 处】

：

中国化学快报（英文版）

【发表日期】

：

2004年期

【关键词】

：

Polyhedral silsesquioxane ferrocene Wittig reaction synthesis 

【基金项目】

：

国家自然科学基金;Key Project of Science and Technology Foundation of Ministry of Education

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论文部分内容阅读

4-(2-Ferrocenylethenyl)-phenyl-POSS Fc-CH=CH-C6H6-(C5H9)7Si8O12 (FEPS, Fc:ferrocene), containing metal and C=C double bond, was firstly synthesized as a mixture of E/Z isomers by the Wittig reaction. The chemical structure of FEPS was characterized by FTIR, 1H-,13C and 29Si- NMR.

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