Stabilizing a severely deformed Al-7Mg alloy with a multimodal grain structure via Mg solute segrega

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Single-phase Al-Mg alloys processed by severe plastic deformation (SPD) usually suffer from unsatis-factory thermal stability at moderate to high temperatures with recrystallization occurring and obvious grain coarsening.In the present work,an Al-7Mg alloy prepared by equal-channel angular pressing(ECAP) possessed markedly enhanced thermal stability upon annealing at moderate to high temperatures(200-275 ℃),compared with those ultrafine-grained dilute Al-Mg alloys with a uniform microstructure.The enhanced thermal stability is due primarily to the multimodal grain structure consisting of nano-,ultrafine-and micron-sized grains,strong segregation and/or clusters of Mg solute along grain bound-aries (GBs),and Al3Mg2 precipitates formed during annealing.First,extensive recovery predominates over recrystallization and consumes most of the stored energy in the ECAPed Al-7Mg alloy annealed at≤ 275 ℃,leading to the recrystallization and growth of nano/ultrafine grains being retarded or post-poned.Moreover,Mg solute segregation and/or clusters along GBs of nano/ultrafine grains could further suppress grain growth via diminishing GB energy and dragging GBs efficiently.In addition,Al3Mg2 pre-cipitates formed with increasing annealing time could inhibit grain growth by pinning GBs.The present multimodal-grained Al-7Mg alloy with enhanced thermal stability is believed to be particularly attractive in potential engineering applications at moderate to high temperatures.
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