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A new macrocycle based on diethoxycarbonyl glycoluril 3,C26H30N6O10,has been synthesized and characterized by single-crystal X-ray diffraction. It crystallizes in monoclinic,space group P21/c with a = 12.7291(10),b = 25.157(2),c = 8.5489(7) ,β = 104.4760(10)°,V = 2650.7(4) 3,Z = 4,C26H30N6O10,Mr = 586.56,F(000) = 1232,T = 292(2) K,Dc = 1.470 g/cm3,μ = 0.115 mm-1,the final R = 0.0590 and wR = 0.1299 for 4918 observed reflections with I > 2σ(I). In the structure of the title compound,a three-dimensional microporous architecture is formed via intermolecular hydrogen bonding interactions.
A new macrocycle based on diethoxycarbonyl glycoluril 3, C26H30N6O10, has been synthesized and characterized by single-crystal X-ray diffraction. It crystallizes in monoclinic space group P21 / c with a = 12.7291 (10), b = 25.157 C = 8.5489 (7) β, β = 104.4760 (10) °, V = 2650.7 (4) 3, Z = 4, C26H30N6O10, Mr = 586.56, F (000) = 1232, T = 292 Dc = 1.470 g / cm3, μ = 0.115 mm-1, the final R = 0.0590 and wR = 0.1299 for 4918 observed reflections with I> 2σ (I). In the structure of the title compound, a three-dimensional microporous architecture is formed via intermolecular hydrogen bonding interactions.