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xMoO2-(1-x)α-Fe2O3 nanoparticle system with molarities x = 0.1, 0.3, 0.5 and 0.7 was successfully synthesized by mechanochemical activation of MoO2 and α-Fe2O3 mixtures for 0 - 12 hours of ball milling time. X-ray powder diffraction (XRD), Mössba