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用HPLC法测定了慢肾宁胶囊中淫羊藿甙的含量,提取用50%乙醇,超声振荡提取20min;线性范围0.062~1.116μg。淫羊藿甙的平均空白加样回收率为99.51%,RSD为0.72%(n=6);样品加样回收率为99.70%。RSD为1.60%(n=6)。方法简便,快速,精密度和稳定性良好,适于慢肾宁胶囊生产的质量控制。
The content of Epimedium in “Wanhening Capsule” was determined by HPLC. The extract was extracted with 50% ethanol and sonicated for 20 min. The linear range was 0.062 to 1.116 μg. The average blank recovery rate of epimedium was 99.51%, RSD was 0.72% (n=6), and the sample recovery rate was 99.70%. The RSD is 1.60% (n=6). The method is simple, rapid, and has good precision and stability. It is suitable for the quality control of the slow kidney capsule production.