Hydrothermal synthesis of monodisperse α-Fe_2O_3 hexagonal platelets

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Uniformly sized α-Fe2O3 hexagonal platelets were synthesized by a hydrothermal process using Fe(OH)3 suspension and large amount of NaOH.The reaction products were characterized by X-ray diffraction(XRD),scanning electron microscopy(SEM),transmission electron microscopy(TEM),selected area electron diffraction(SAED),and a vibrating sample magnetometer(VSM).The results show that the hexagonal platelets are fine,monodisperse and consisting of single-crystals.The magnetic hysteresis(M-H) curve of the samples measured at room temperature indicates that the α-Fe2O3 micro-platelets exhibit ferromagnetic behaviors with relatively low coercivity. Uniformly sized α-Fe2O3 hexagonal platelets were synthesized by a hydrothermal process using Fe (OH) 3 suspension and large amount of NaOH. The reaction products were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), selected area electron diffraction (SAED), and a vibrating sample magnetometer (VSM). The results show that the hexagonal platelets are fine, monodisperse and consisting of single-crystals. The magnetic hysteresis (MH) curve of the samples measured at room temperature indicates that the α-Fe2O3 micro-platelets exhibit ferromagnetic behaviors with relatively low coercivity.
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