Fabrication and Magnetic Properties of Composite Ni_(0.5)Zn_(0.5)Fe_2O_4/Pb(Zr_(0.52)Ti_(0.48))O_3 N

来源 :Journal of Wuhan University of Technology(Materials Science | 被引量 : 0次 | 上传用户:furong2599
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One-dimensional and quasi-one-dimensional nanostructure materials are promising building blocks for electromagnetic devices and nanosystems.In this work,the composite Ni0.5Zn0.5Fe2O4(NZFO)/ Pb(Zr0.52Ti0.48)O3(PZT) nanofibers with average diameters about 65 nm are prepared by electrospinning from poly(vinyl pyrrolidone) (PVP) and metal salts.The precursor composite NZFO/PZT/PVP nanofibers and the subsequent calcined NZFO/PZT nanofibers are investigated by Fourier transform infrared spectroscopy (FT- IR) ,X-ray diffraction (XRD),scanning electron microscopy (SEM).The magnetic properties for nanofibers are measured by vibrating sample magnetometer(VSM).The NZFO/PZT nanofibers obtained at calcination temperature of 900 °C for 2 h consist of the ferromagnetic spinel NZFO and ferroelectric perovskite PZT phases,which are constructed from about 37 nm NZFO and 17 nm PZT grains.The saturation magnetization of these NZFO/PZT nanofibers increases with increasing calcination temperature and contents of NZFO in the composite. One-dimensional and quasi-one-dimensional nanostructure materials are promising building blocks for electromagnetic devices and nanosystems. In this work, the composite Ni0.5Zn0.5Fe2O4 (NZFO) / Pb (Zr0.52Ti0.48) O3 (PZT) nanofibers with average diameters about 65 nm are prepared by electrospinning from poly (vinyl pyrrolidone) (PVP) and metal salts. The precursor composite NZFO / PZT / PVP nanofibers and the subsequent calcined NZFO / PZT nanofibers are investigated by Fourier transform infrared spectroscopy The magnetic properties for nanofibers were measured by vibrating sample magnetometer (VSM). The NZFO / PZT nanofibers obtained at calcination temperature of 900 ° C for 2 h consist of the ferromagnetic spinel NZFO and ferroelectric perovskite PZT phases, which are constructed from about 37 nm NZFO and 17 nm PZT grains. The saturation magnetization of these NZFO / PZT nanofibers increases with increasing calcination temperature and conte nts of NZFO in the composite.
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