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A new dinuclear copper(Ⅱ) complex (Cu(C12H17N2O)(NCS)2, C26H34Cu2N6O2S2) has been synthesized and characterized by X-ray structure determination. It crystallizes in the triclinic system, space group P1^- with a = 11.289(2), b = 12.071(2), c = 12.113(2)A