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(n-Bu_4N)_3W_2Cl_9, prepared from K_3W_2Cl_9, can be readily converted to a series of [W(IV)]cluster compounds,W_3Cl_4(μ-OR)_2(OR’)_2(R’OH)_2, including seven known compounds and two newcompounds with R=Me, R＇=i-Pr and sec-Bu. The crystallographic data of 7 and 8 are herebypresented.