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建立了分析以2-氮-2,4,4-三甲基戊烷与1,1-二苯乙烯之间的阳离子反应作为异丁烯阳离子聚合模型反应产物的高效液相色谱方法,测定了上述模型反应各平衡组分浓度。所用的色谱柱为CLC-Ph(苯基全多孔硅胶键合相)直径6.0mm×150mm,流动相为甲醇-水(85.5:14.5)。应用此方法成功地测试了近800个样品。
A high performance liquid chromatographic method was developed for the analysis of the cationic reaction between 2-aza-2,4,4-trimethylpentane and 1,1-stilbene as the reaction product of isobutylene cationic polymerization model. The above model The reaction of the equilibrium component concentration. The column used was CLC-Ph (phenyl fully porous silica bonded phase) with a diameter of 6.0 mm × 150 mm and a mobile phase of methanol-water (85.5: 14.5). Nearly 800 samples have been successfully tested using this method.