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本实验用南京分析仪器厂 CX-801型国产高压液相色谱仪以簿壳玻球-烷基(Permapha-se ODS)为填料,甲醇-水为流动相,反相分配法分离了大黄蒽醌类化合物。Permaphase ODS 与天津化学试剂厂生产的薄壳玻球(1)-烷基,上海试剂厂生产的薄壳玻球-烷基为同品种填料,可应用于稠环芳香化合物、核酸类、脂溶性维生素、甾体激素化合物、除虫菊酯等的分离。本实验用于分离大黄蒽醌类化合物。
In this experiment, Nanjing Analytical Instrument Factory CX-801 domestic high-pressure liquid chromatograph was used as the packing material, the methanol-water mobile phase was used as the mobile phase, and the reversed-phase distribution method was used to separate rhubarb. Compounds. Permaphase ODS and (1)-alkyl thin-shell glass ball produced by Tianjin Chemical Reagent Factory, and the thin-shell glass ball-alkyl group produced by Shanghai Reagent Factory are the same kind of fillers, can be applied to condensed ring aromatic compounds, nucleic acids, fat-soluble Separation of vitamins, steroid hormone compounds, pyrethrins, and the like. This experiment was used to isolate rhubarb compounds.