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对在微波催化条件下邻苯二酚和氯代异丁烯单醚化反应进行了研究 ,考察了各种不同碱、相转移催化剂、溶剂、微波功率和反应时间对反应的影响。邻异丁烯氧基苯酚的收率由常规方法的 5 4%提高到 6 8% ,反应速率是常规方法的 1 2 0倍。
Under the microwave catalytic conditions, the catechol and chloroisobutylene monoetherification reactions were investigated, and the effects of various alkali, phase transfer catalyst, solvent, microwave power and reaction time on the reaction were investigated. The yield of o-isobuteneoxyphenol was increased from 54% to 68% of the conventional method, and the reaction rate was 120 times higher than that of the conventional method.