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研究了室温下在含有少量水的ＮｄＣｌ３－ＮｉＣｌ２－ＤＭＦ溶液中电沉积制备Ｎｄ－Ｎｉ功能合金膜，选定一系列的阴极电位进行恒电位电解，制备出不同Ｎｄ含量的Ｎｄ－Ｎｉ合金膜．ＥＤＡＸ和ＸＲＤ分析表明：在０．１０ｍｏｌ／ｄｍ３ＮｄＣｌ３＋０．１０ｍｏｌ／ｄｍ３ＮｉＣｌ２的ＤＭＦ溶液中，控制电位为－１．７５Ｖ（对ＳＣＥ）进行恒电位电解，可得到有金属光泽、附着力强的银白色Ｎｄ－Ｎｉ合金膜
Nd-Ni alloy films were prepared by electrodeposition of NdCl3-NiCl2-DMF solution containing a small amount of water at room temperature. A series of cathodic potentials were selected for potentiostatic electrolysis to prepare Nd-Ni alloy films with different Nd contents. EDAX and XRD analysis showed that the control potential of -1.75V (SCE) was potentiostatic electrolysis in 0.10mol / dm3NdCl3 + 0.10mol / dm3NiCl2 DMF solution to obtain a silver-white Nd -Ni alloy film