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本文用定向选择的方法,研究了在20K下测定的~(15)N-~(63)Cu-HAP的5:1DMSO-EtOH溶液ENDOR谱,精确测得配体~(15)核的各向异性超超精细耦合张量值和各种不等价~1H核的超超精细耦合张量值.研究结果表明,我们前文的波谱解析,方法是正确的,数据是可靠的.
In this paper, we studied the ENDOR spectra of 5: 1DMSO-EtOH solution of ~ (15) N- ~ (63) Cu-HAP measured at 20K with the method of directional selection. The results show that our method of spectral analysis is correct, and the data is reliable. Key words: super-hyperfine coupling tensor;