本文报道了用内标法对六神丸、安宫牛黄散及安宫牛黄丸中麝香所含之麝香酮的气相色谱分析。作者在设定条件下,以正十九烷为内标,测定了麝香酮的定量校正因子。比较了提取及提取后浓缩两种方法的测定结果。通过回收率实验和样品测定表明,本法适用于某些中成药中麝香酮的定量测定,可用于中成药内在质量控制。 This article reported the gas chromatographic analysis of musk ketone contained in Liuxiang Pill, Angong Niuhuang Powder and Angong Niuhuang Pills using internal standard method. Under the set conditions, the authors measured n-nonadecane as an internal standard and determined the quantitative correction factor of muskone. The results of the two methods of extraction and extraction and concentration were compared. Through the recovery experiment and sample determination, this law is applicable to the quantitative determination of musk ketone in some proprietary Chinese medicines and can be used for the inherent quality control of proprietary Chinese medicines.