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Crystal structures of neodymium (Ⅲ) and dysprosium (Ⅲ) nitrate complexes with the new ligand N, N'-dimethyl-N, N'-diphenyladipamide (mpaa) has been determined. Both complexes are triclinic with space group Pi ,formula [C22H30N5NdO12S]2 1 [C42H54N7