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目的 :建立华海乙肝泡腾颗粒剂的质量标准。方法 :采用薄层色谱法对华海乙肝泡腾颗粒剂进行定性鉴别 ;并应用高效液相色谱法对其中的五味子乙素进行含量测定。结果 :薄层色谱均能检出黄芪、柴胡、虎杖、五味子 ;五味子乙素在0 .848～ 4.2 40 μg范围内线性关系良好 ,r =0 .9999,平均回收率 98.19%,RSD =1.12 %。 结论 :此法可作为控制华海乙肝泡腾颗粒剂质量的方法。
Objective : To establish the quality standard of Huahai Yipeng Effervescent Granules. Methods: The qualitative identification of Huahai Yipeng Effervescent granules was performed by thin-layer chromatography. The content of schizandrin B was determined by high performance liquid chromatography. Results: TLC could detect Astragalus, Bupleurum, Polygonum cuspidatum and Schisandra chinensis. The linear relationship was good in the range of 0.848-4.2 40 μg, r=0.9999, the average recovery rate was 98.19%, and RSD was 1.12. %. Conclusion : This method can be used as a method to control the quality of Hua Hai Yi Gan Effervescent Granules.