通过在含有SeSO32-和Cd2+的室温水溶液中,用模板-电沉积法在纳米孔阵列阳极氧化铝膜(AAM)模板中制备了高有序性的CdSe纳米线阵列,并对其形貌、结构和组分进行了表征。扫描电子显微镜(SEM)和透射电子显微镜(TEM)结果表明,纳米线阵列中的CdSe纳米线具有相同的长度和直径,分别对应于使用的AAM模板的厚度和孔径;X-射线衍射(XRD)和X-射线能谱(EDAX)结果表明,CdSe纳米线中Cd和Se的化学组成非常接近于1∶1,其结构为立方CdSe。另外,对模板-电沉积法制备CdSe纳米线的机理进行了讨论。 A highly ordered array of CdSe nanowires was prepared in a nanoporous array anodic aluminum oxide (AAM) template by a template-electrodeposition method in aqueous solution containing SeSO32- and Cd2 + at room temperature. The morphology, structure And components were characterized. Scanning electron microscopy (SEM) and transmission electron microscopy (TEM) results show that the CdSe nanowires in the nanowire arrays have the same length and diameter, respectively corresponding to the thickness and pore size of the AAM template used; X-ray diffraction (XRD) And EDAX results show that the chemical composition of Cd and Se in CdSe nanowires is very close to 1: 1 and the structure is cubic CdSe. In addition, the mechanism of template-electrodeposition CdSe nanowires was discussed.