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C6H12N4Br4Ag4,Mr = 891.31, orthorhombic, Pnma, a = 8.778(2),b = 9.80.5(2), c = 16.906(3) A, V = 1455.1(4) A3, Z = 4, Dx = 4.069, Dm (displacement of H2O) = 4.03 g cm-3 , A(Mo-Ka) = 161.3 cm-1 , F(OOO) = 1615.77,T = 295°, final R = 0.052 arid Rw = 0.062 for 1472 observed reflections.All four lone pairs of each (CH2)6N4 molecule serve as ligand sites in a polymeric framework comprising octahedral AgBr5N, tetrahedral AgBr3N, and tetragonal pyramidal AgBr4N coordination polyhedra. The Ag-N and Ag-Br bond lengths lie in the ranges 2.366(12)-2.454(12) and 2.640(2)-3.178(2) A, respectively.
A = 8.781 (2), b = 9.80.5 (2), c = 16.906 (3) A, V = 1455.1 (4) A3, Z = 4, Dx = 4.069, Dm (displacement of H2O) = 4.03 g cm-3, A (Mo-Ka) = 161.3 cm -1, F (OOO) = 1615.77, T = 295 °, final R = 0.052 arid Rw = 0.062 for 1472 observed reflections. All four lone pairs of each (CH2) 6N4 molecule serve as a ligand site in a polymeric framework comprising octahedral AgBr5N, tetrahedral AgBr3N, and tetragonal pyramidal AgBr4N coordination polyhedra. The Ag-N and Ag-Br bond lengths lie in the ranges 2.366 (12 ) -2.454 (12) and 2.640 (2) -3.178 (2) A, respectively.