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The title compound C2N5H6+C6N3O7H2-was synthesized by the reaction of 3,5-diamino-1,2,4-triazole and picric acid in the mixture of ethanol and water solution.Single crystals suitable for X-ray measurement were obtained at room temperature.The structure was characterized by elemental analysis and IR and determined by X-ray diffraction analysis.Crystallographic data:C8N8H8O7,Mr = 328.22,monoclinic,space group C2/c with a = 22.815(2),b = 4.8086(5),c = 22.564(2),β = 93.976(2)°,V = 2469.6(4)3,Dc = 1.766 g/cm3,Z = 8,μ = 0.156 mm-1,F(000) = 1344,the final R= 0.0309,wR= 0.0864.
The title compound C2N5H6 + C6N3O7H2-was synthesized by the reaction of 3,5-diamino-1,2,4-triazole and picric acid in the mixture of ethanol and water solution. Single crystals suitable for X-ray measurement were obtained at room temperature.The structure was characterized by elemental analysis and IR and determined by X-ray diffraction analysis. Crystallographic data: C8N8H8O7, Mr = 328.22, monoclinic, space group C2 / c with a = 22.815 (2), b = 4.8086 (5) , C = 22.564 (2) β, β = 93.976 (2) °, V = 2469.6 (4) 3, Dc = 1.766 g / cm3, Z = 8, μ = 0.156 mm-1, F , the final R = 0.0309, wR = 0.0864.