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乙酰基二茂铁是按付氏酰基化反应制备的,在CH_2Cl_2溶剂中培养得到血红色柱状晶体,经元素分析及结构分析共分子式为C_(12)H_(12)OFe。在CAD4-四园衍射仪上用Mo K_a射线以θ—2θ扫描在3°≤2θ≤56°范围收集衍射数据,经LP因子及经验
Acetylferrocene is prepared by the Friedel-Crafts acylation reaction, and the blood-red columnar crystals are obtained by the CH_2Cl_2 solvent. The elemental analysis and structural analysis show that the molecular formula is C_ (12) H_ (12) OFe. Diffraction data were collected on a CAD 4-Siyuan diffractometer with a Mo K_a ray at a θ-2θ scan in the range of 3 ° ≦ 2θ ≦ 56 °. The LP factor and the experience