按照文献［１］进行水中挥发酚的测定时，要求实验用水均为无酚水，但无酚水的配制过程既费时费力，且分析成本相应也高。文献［２］中介绍用新制蒸馏水代替无酚水，同样耗电耗时。我们采用新接的去离子水作为分析用水，经实验证明，结果满意，方法可行。１实验部分１．１... According to the literature [1] for the determination of volatile phenol in water, the experimental water is required to be phenol-free water, but the process of preparation without phenol water is time-consuming and labor-intensive, and the analysis cost is correspondingly high. Literature [2] describes the use of new distilled water instead of phenol-free water, the same time-consuming power consumption. We use the new accession of deionized water as the analysis of water, the experiment proved that the results are satisfactory, the method is feasible. 1 Experimental Section 1.1 ...