舒乐宁洗剂的薄层鉴别和含量测定

来源 :中药新药与临床药理 | 被引量 : 0次 | 上传用户:intaaac
下载到本地 , 更方便阅读
声明 : 本文档内容版权归属内容提供方 , 如果您对本文有版权争议 , 可与客服联系进行内容授权或下架
论文部分内容阅读
采用TLC法对舒乐宁洗剂中地肤子及蛇床子进行了定性鉴别,薄层扫描法测定苦参碱及盐酸小檗碱含量。苦参碱在1.0~5.0μg范围内线性关系良好,平均回收率为98.52%,RSD为0.81%;盐酸小檗碱在1.1~5.5μg范围内线性关系良好,平均回收率为97.63%,RSD为1.88%。 The qualitative identification of Kochia scoparia and Cnidium monnieri in ShuLing Ning lotion was carried out by TLC, and the content of matrine and berberine hydrochloride was measured by TLC scanning. The calibration curve showed good linearity in the range of 1.0-5.0 μg. The average recovery was 98.52% and the RSD was 0.81%. The berberine hydrochloride had good linearity in the range of 1.1-5.5 μg. The average recovery was 97.63%. The RSD was 1.88%.
其他文献
用PR-HPLC法测定丁公藤注射液有效成分总东莨菪内酯在小鼠血浆中的浓度。色谱条件:SpheriSorb_C18不锈钢柱,流动相为甲醇-水-冰醋酸(38∶62∶0.19),检测波长345nm。血浆样品
期刊
建立了HPLC测定复方珍珠口疮颗粒中没食子酸含量的方法,测定制剂中没食子酸含量为3.9%,明显高于生产用原料五倍子药材中没食子酸含量的2.8%,主要系生产过程中五倍子鞣质水解