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[Et4N]2 [WCu3S4 (S2CNEt2)3], Mr = 1172. 01, orthorhombic, space group P212121 with a=12. 858(9),b=13. 204(5) ,c=29. 501(9) A ,V=5008. 7 A3, Z = 4, Dc = 1. 55gcm-3, μ(MoKa) = 40. 3cm-1. The final R and Rw are 0. 069 and 0. 075, respectively, for 3072 observed unique reflections. The anion contains a slightly distorted WS42~ tetrahedron coordinated by three CuS2 CNEt2 units,with four metal atoms lying in a plane.
(Et4N) 2 [WCu3S4 (S2CNEt2) 3], Mr = 1172.01, orthorhombic, space group P212121 with a = 12.8588, b = 13.204 5, c = A, V = 5008. 7 A3, Z = 4, Dc = 1. 55gcm-3, μ (MoKa) = 40. 3cm-1. The final R and Rw are 0. 069 and 0. 075, respectively, for 3072 observed unique reflections. The anion contains a slightly distorted WS42 ~ tetrahedron coordinated by three CuS2 CNEt2 units, with four metal atoms lying in a plane.