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Crystal of the title complex, C 44 H 41 ClP 2Ru, belongs to monoclinic system, space group P2 1/n, a=11.968(2), b=17.721(2), c=17.322(2), β=97^669(12)°, V=3640.8(9) 3, M r=768.2, Z=4, D c =1.402g.cm -3 , μ =5^217mm -1 , F (000)=1584, the final R =0.0418 and R w =0.0551 for 3734 observed reflections ( F>3.9σ(F )). The geometry around the ruthenium can be considered as a distorted tetrahedron. The electronic and steric effects of iso propyl substituent on the structure of the title complex(I) are discussed.
Crystal of the title complex, C 44 H 41 ClP 2Ru, belongs to monoclinic system, space group P2 1 / n, a = 11.968 (2), b = 17.721 (2), c = 17.322 669 (12) °, V = 3640.8 (9) 3, M r = 768.2, Z = 4, D c = 1.402g.cm -3, μ = 5 ) = 1584, the final R = 0.0418 and R w = 0.0551 for 3734 observed reflections (F> 3.9σ (F)). The geometry around the ruthenium can be considered as a distorted tetrahedron. The electronic and steric effects of iso propyl substituent on the structure of the title complex (I) are discussed.