The corrosion behavior of nano-meter embedded phase in Ti implanted H13 steel

来源 :Science in China(Series E:Technological Sciences) | 被引量 : 0次 | 上传用户:naruto_Dragonballlll
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On the SEM micrographs of Ti implanted H13 steel, a tree-branch-like structure can be observed. Further investigation with TEM shows that the newly tormed composition is a formation of nann-meter FeTi_2 phase in Ti implanted layer. The layer with a relatively high corrosion resistance has been formed in Ti implanted H13 steel with this structure.The results of electrochemical measurement show that the corrosion current density decreases obviously with an increase of ion dose. The corrosion current density in Ti implanted steel with a dose of 1.3×10~(18)/cm~2 is 8-20 times less than that of Ti implanted steel with a dose of 6×10~(17)/cm~2. The corrosion behavior of Ti implanted steel with a dose of 6×10~(17)/cm~2 could be further improved as the sample was annealed at 500℃ for 20 min and the corrosion current density decreases by 48-80 times compared to that of non-implanted samples. The corrosion trace was not observed on the annealing sample by SEM, after multi-sweep cyclic voltammetry of 40 cycles On the SEM micrographs of Ti implanted H13 steel, a tree-branch-like structure can be observed. Further investigation with TEM shows that the newly tormed composition is a formation of nann-meter FeTi_2 phase in Ti implanted layer. The layer with a relatively high corrosion resistance has been formed in Ti implanted H13 steel with this structure. The results of electrochemical measurement show that the corrosion current density decreased obviously with an increase of ion dose. The corrosion current density in Ti implanted steel with a dose of 1.3 × 10 ~ (18) / cm ~ 2 is 8-20 times less than that of Ti implanted steel with a dose of 6 × 10-17 / cm ~ 2. The corrosion behavior of Ti implanted steel with a dose of 6 × 10 ~ (17) / cm ~ 2 could be further improved as the sample was annealed at 500 ° C for 20 min and the corrosion current density decreases by 48-80 times compared to that of non-implanted samples. The corrosion trace was not observed on the annealing sample by SEM, after multi-sweep cyclic volta mmetry of 40 cycles
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