,Synthesis of α-amino-β-keto-esters (β-oxodipeptides)

来源 :中国高等学校学术文摘·化学 | 被引量 : 0次 | 上传用户：A88851258

【摘要】

：

The synthesis of α-amino-β-keto-esters (β-oxo dipeptides) was studied. Corresponding α-amino-β-keto-esters were prepared from BOC-(L)-Valine and BOC-(L)-is

【作者】

：

Yanjie XU Ligong CHEN

【机构】

：

School of Chemical Engineering and Technology,Tianjin University,Tianjin 300072,China

【出处】

：

中国高等学校学术文摘·化学

【发表日期】

：

2008年4期

【关键词】

：

α-amino-β-keto-esters dipeptide oxidation Dess-Martin Periodinane (DMP)

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The synthesis of α-amino-β-keto-esters (β-oxo dipeptides) was studied. Corresponding α-amino-β-keto-esters were prepared from BOC-(L)-Valine and BOC-(L)-isoleucine by coupling with (D,L)-threonine hydro-chloride and oxidation with Dess-Martin periodinane (DMP) with a total yield of 48% and 38%, respectively.

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,Synthesis of α-amino-β-keto-esters (β-oxodipeptides)

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