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The title compound (4,4′-H2bipy)[CdBr4]·H2O 1 has been synthesized via hydrothermal reaction and characterized by X-ray diffraction. The crystal belongs to monoclinic,space group P21/c with a=8.260(3),b=23.926(7),c=9.774(2),β=106.777(9)o,C10H12Br4CdN2O,Mr=608.26,V=1849.4(9)3,Z=4,Dc=2.185 g/cm3,S=1.005,μ(MoKα) =9.814 mm–1,F(000)=1128,R=0.0646 and wR=0.0989. The crystal structure analysis of 1 reveals that the title compound features an isolated structure,based on discrete 4,4′-H2bipy moieties and lattice water molecules which are linked by hydrogen bonds together with tetra-hedral cadmium atoms terminally coordinated by four bromine atoms.
The title compound (4,4’-H2bipy) [CdBr4] .H2O 1 has been synthesized via hydrothermal reaction and characterized by X-ray diffraction. The crystal belongs to monoclinic, space group P21 / c with a = 8.260 B = 23.926 (7), c = 9.774 (2) β, β = 106.777 (9) o, C10H12Br4CdN2O, Mr = 608.26, V = 1849.4 (9) 3, Z = 4, Dc = 2.185 g / cm3, S = 1.005, μ (MoKα) = 9.814 mm -1, F (000) = 1128, R = 0.0646 and wR = 0.0989. The crystal structure analysis of 1 reveals that the title compound features an isolated structure, ’-Hbbipy moieties and lattice water molecules which are linked by hydrogen bonds together with tetra-hedral cadmium atoms terminally coordinated by four bromine atoms.