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本文介绍电子探针分析用单质金属标准样品的制作方法。其中包括:①电子探针分析对标准样品的要求。②单质金属标准样品材料的制备方法。包括:材料的熔炼,杂质的检验,加工成形等。③标准样品的制作方法。包括:样品柱和样品座的设计,样品与样品柱之间的接合,样品工作面的研磨和抛光等。④标准样品的检验方法。包括:平面性,粗糙度,均匀性,稳定性,污染等。文中还介绍了自己研制的几种单质金属标准样品,以及部分检验数据。
This article describes the preparation of single-metal standard sample for electron probe analysis. Including: ① electronic probe analysis of the standard sample requirements. ② single-metal standard sample preparation methods. Including: smelting of materials, inspection of impurities, processing and forming. ③ standard sample production methods. Including: sample column and sample holder design, sample and sample column between the joint, the sample surface grinding and polishing. ④ standard test methods. Including: flatness, roughness, uniformity, stability, pollution and so on. The article also introduced his own research and development of several simple metal standard samples, as well as some test data.