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Three metal molybdate hydrates,Fe(H2O) 2(MoO4)2·H3O(FeMo),NaCo 2(MoO4) 2(H3O2)(CoMo) and Mn 2(MoO4)3·2H3O(MnMo),were synthesized by the mixed-solvent-thermal methods and characterized by singlecrystal X-ray diffraction.X-Ray photoelectron spectr