【摘 要】
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The title compound, methyl 2-(diphenylamino)-4-phenyl-1,3-thiazole-5-carboxylate, was synthesized and studied by single-crystal X-ray diffraction method. The st
【机 构】
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Department of Chemistry, Urmia Branch, Islamic Azad University, P. O. Box 969, Urmia, Iran,Departmen
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The title compound, methyl 2-(diphenylamino)-4-phenyl-1,3-thiazole-5-carboxylate, was synthesized and studied by single-crystal X-ray diffraction method. The structure of the product was confirmed by IR, 1H- and 13C-NMR spectroscopy and elemental analysis. These experimental studies were supported by quantum mechanical calculations. The structure was solved in monoclinic, space group P21/c with a = 9.573(3), b = 19.533(7), c = 9.876(3), β = 92.35(4)°, V = 1845.2(10)3, T = 85(2) K, Z = 4, R = 0.040 and wR = 0.089 for 6424 observed reflections withI>2σ(I).
The title compound, methyl 2- (diphenylamino) -4-phenyl-1,3-thiazole-5-carboxylate, was synthesized and studied by single-crystal X-ray diffraction method. The structure of the product was confirmed by IR, These structures were solved in monoclinic, space group P21 / c with a = 9.573 (3), b = 19.533 (7), c = 9.876 (3) β, β = 92.35 (4) °, V = 1845.2 (10) 3, T = 85 (2) K, Z = 4, R = 0.040 and wR = 0.089 for 6424 observed reflections with I> 2σ ).
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