Silver-palladium alloy deposited by DC magnetron sputtering method as lubricant for high temperature

来源 :Transactions of Nonferrous Metals Society of China | 被引量 : 0次 | 上传用户:valgrind2
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The silver-palladium(Ag-Pd) alloy coating as a solid lubricant was investigated for its application to the high temperature stud bolts used in nuclear power plants.A hex bolt sample was prepared in the following steps:1) bolt surface treatment using alumina grit blasting for cleaning and increasing the surface area;2) nickel(Ni) film coating as a glue layer on the surface of the bolt;and 3) Ag-Pd alloy coating on the Ni film.The films were deposited by using a direct current(DC) magnetron sputtering system.The thickness and composition of the Ag-Pd alloy film have effect on the friction coefficient,which was determined using axial force measurement.A 500 nm-thick Ag-Pd(80-20,molar ratio) alloy film has the lowest friction coefficient of 0.109.A cyclic test was conducted to evaluate the durability of bolts coated with either the Ag-Pd(80-20) alloy film or N-5000 oil.In a cycle,the bolts were inserted into a block using a torque wrench,which was followed by heating and disassembling.After only one cycle,it was not possible to remove the bolts coated with the N-5000 oil from the block.However,the bolts coated with the Ag-Pd(80-20) alloy could be easily removed up until 15 cycles. The silver-palladium (Ag-Pd) alloy coating as a solid lubricant was investigated for its application to the high temperature stud bolts used in nuclear power plants. A hex bolt sample was prepared in the following steps: 1) bolt surface treatment using alumina grit blasting for cleaning and increasing the surface area; 2) nickel (Ni) film coating as a glue layer on the surface of the bolt; and 3) Ag-Pd alloy coating on the Ni film. (DC) magnetron sputtering system. The thickness and composition of the Ag-Pd alloy film have effect on the friction coefficient, which was determined using axial force measurement. A 500 nm-thick Ag-Pd (80-20, molar ratio) alloy film has the lowest friction coefficient of 0.109.A cyclic test was conducted to evaluate the durability of bolts coated with either the Ag-Pd (80-20) alloy film or N-5000 oil.In a cycle, the bolts were inserted into a block using a torque wrench, which was followed by heating and disassembling. Aff r only one cycle, it was not possible to remove the bolts coated with the N-5000 oil from the block.
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