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The title compound l-benzyl-5-((4-methoxyphenyl)ethynyl)-4-phenyl-1H-1,2,3-triazole(C_(24)H_(19)N_3O) was designed and synthesized using one-pot strategy and structural characterization was done by single-crystal X-ray diffraction,NMR,IR and MS.This compound was crystallized out from an ethanolic solution in triclinic system,space group P1 with a =9.9038(9),b = 10.2928(9),c = 18.8715(19) ?,α = 103.541(6),β = 90.507(7),γ = 97.157(7)°,V =1854.2(3) ?~3,Z = 4,crystal size(mm) = 0.25 × 0.1 × 0.1 and R_(int) = 0.068.Its asymmetric unit contains two independent molecules.The crystal structure of the title compound is stabilized by intramolecular interactions of types C-H…N and C-H…O.Additionally,X-ray analysis reveals obvious C-H…π,π-π stacking interactions between two adjacent aromatic ring planes.
The title compound l-benzyl-5 - ((4-methoxyphenyl) ethynyl) -4-phenyl-1H- 1,2,3-triazole (C 24 H 19 N 3 O) was designed and synthesized using one-pot strategy and structural characterization was done by single-crystal X-ray diffraction, NMR, IR and MS. This compound was crystallized out from an ethanolic solution in triclinic system, space group P1 with a = 9.9038 (9), b = 10.2928 ), c = 18.8715 (19)?,? = 103.541 (6),? = 90.507 (7),? = 97.157 (7) °, V = 1854.2 ) = 0.25 × 0.1 × 0.1 and R_ (int) = 0.068.Its asymmetric unit contains two independent molecules. The crystal structure of the title compound is stabilized by intramolecular interactions of types CH ... N and CH ... O.Additionally, X-ray analysis reveals obvious CH ... π, π-π stacking interactions between two adjacent aromatic ring planes.