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A novel platinum(Ⅳ) complex [Ph3PEt]2[PtCl6] 1 obtained from the reaction of H2PtCl6 and [Ph3PEt]I (Ph3PEt+ = ethyl-triphenylphosphenonium) has been structurally characterized.It crystallizes in triclinic, space group P1 with a = 10.20850(10), b = 10.3387