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三氯蔗糖是使用范围较广的高甜度甜味剂，工业生产时需要对氯代反应进行后处理，应用科学工艺可提升收率。阐述了工艺改进的原理，重点分析后处理条件差异与收率影响，进而得到最佳工艺结论，以供行业生产参考。“,” Sucralose is a wide range of high-sweetness sweeteners. In industrial production, the chlorination reaction needsto be post-treated, and the application of scientific technology can increase the yield. This study expounded the principle of process improvement, detailed the research process, focused on analyzing the difference in post-processing conditions and the impact of yield, and then obtained the best process conclusion for industry production reference.