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The single crystal X-ray diffraction data of (2,4-(CH3)2C5H5]2VCO have been collected under low temperature (-60℃) and the crystal structure has been solved by heavy atom method. It belongs to orthorhombic system, space group P212121, a =9.921(6), b =9.899(6), c=14.491(8) A, Z=4. Several cycles of block matrix least-squares refinement gave the final R=0.087.
The single crystal X-ray diffraction data of (2,4- (CH3) 2C5H5] 2VCO has been collected under low temperature (-60 ° C) and the crystal structure has been solved by heavy atom method. It belongs to orthorhombic system, space group P212121, a = 9.921 (6), b = 9.899 (6), c = 14.491 (8) A, Z = 4. Several cycles of block matrix least-squares refinement gave the final R = 0.087.