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通过对预充氢310不锈钢薄膜在透射电镜(TEM)下的原位拉伸观察,并和不含氢试样的结果相比较,研究了氢在韧-脆转变中的作用及氢致脆断机理.结果表明,预充氢的310不锈钢试样在拉伸过程中从裂尖发射大量位错,平衡后形成无位错区(DFZ);纳米级微裂纹择优在DFZ中形核;微裂纹不钝化为空洞,而是通过多个微裂纹的形核及相互连接导致裂纹的脆性扩展.即氢使奥氏体不锈钢由韧变脆的根本原因是氢抑制了DFZ中纳米级微裂纹向空洞的转化.
The effect of hydrogen on the ductile-brittle transition and hydrogen-induced brittle fracture were studied by observing the in-situ tension of the pre-hydrogenated 310 stainless steel thin film under transmission electron microscope (TEM) mechanism. The results show that a large number of dislocations are emitted from the crack tip during the pre-hydrogenation of 310 stainless steel sample, and the dislocation-free region (DFZ) is formed after the equilibration. The nano-scale microcracks preferentially nucleate in the DFZ; the microcracks are not blunt Into a hollow, but through a number of micro-crack nucleation and interconnection led to brittle fracture expansion. The fundamental reason that hydrogen makes austenitic stainless steel brittle from ductile is that hydrogen suppresses the transformation of nano-scale microcracks to cavities in DFZ.