本文以喷涂抗静电剂与微量镀金的方法,利用SEM和SALS研究了等规聚丙烯球晶的拉伸形变过程,克服了单独使用抗静电剂和单独镀金方法的缺点。在观察过程中,二次电子信号强,试样无放电现象,也无金膜龟裂现象。研究结果表明:圆形球晶在拉伸应力作用下逐渐变为椭圆形,球晶中的径向微纤向赤道方向滑移取向。 In this paper, by means of spraying antistatic agent and micro-plating gold, SEM and SALS were used to study the tensile deformation process of isotactic polypropylene spherulites and overcome the disadvantages of using antistatic agent alone and gold plating alone. In the observation process, the secondary electronic signal is strong, no discharge phenomenon of the sample, nor the phenomenon of gold film cracking. The results show that the spherical spherulites gradually become elliptical under the tensile stress, and the radial microfibers in the spherulites slip toward the equator.