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目的 建立五虎散的质量标准。方法 采用 TL C法对处方中当归、白芷、红花进行定性鉴别 ;采用 HPL C法测定升麻苷和 5 - O-甲基维斯阿米醇苷的含量。结果 升麻苷在 0 .370 0～ 1.85 0 0 μg,5 - O-甲基维斯阿米醇苷在0 .1910～ 0 .95 5 0μg与峰面积具有良好的线性关系 ;平均回收率分别为 10 0 .74 %和 98.33% ,RSD分别为 0 .6 7%和 1.91% (n=5 )。结论 建立的方法简便、准确、可靠 ,可作为控制该药品的质量标准。
Objective To establish the quality standard of Wuhu Powder. Methods The TL C method was used to qualitatively identify Angelica sinensis, Radix Paeoniae Rubra and Radix Scutellariae in the formulation, and HPL C method was used to determine the content of Cimicifolium and 5 -O-Methylvisanaminoside. Results There was a good linear relationship between the amount of ricinin at 0.370 to 1.85 0 μg and 5-O-methylstilbenidoside at the range of 0.1910 to 0.995 50 μg. The average recoveries were It was 100.74% and 98.33%, respectively, with RSDs of 0.67% and 1.91% (n=5). Conclusion The established method is simple, accurate and reliable and can be used as a quality control standard for the drug.