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本文以琥珀酸二异辛酯磺酸钠(AOT)/水/异辛烷反相胶束体系为研究对象,利用电导率仪、红外光谱、核磁共振、差示扫描量热(DSC)等手段,研究了反相胶束微反应器的总体结构和内核水的特征,讨论了温度以及不同类型的有机添加物对体系的影响,总结了制备纳米微粒的适宜条件。在此基础上进行了ZnS纳米微粒的制备,通过透射电镜和紫外光谱考察了制得的纳米微粒。
In this paper, AOT / water / isooctane reverse micellar system of succinic acid was used as the research object. By means of conductivity meter, infrared spectroscopy, nuclear magnetic resonance and differential scanning calorimetry (DSC) , Studied the overall structure of the micellar microreactor and the characteristics of the core water. The effects of temperature and different types of organic additives on the system were discussed. The suitable conditions for preparing the nanoparticles were summarized. On this basis, ZnS nanoparticles were prepared. The prepared nanoparticles were characterized by transmission electron microscopy and ultraviolet spectroscopy.