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本文提出一个使用玻碳薄汞膜电极测定氟哌酸的伏安法．在ｐＨ５．６～７的乙酸～乙酸钠缓冲溶液中，氟哌酸在－１５００ｍｖ有一个灵敏的导数阴极波，用于胶囊中氟哌酸含量的测定，结果满意．氟哌酸浓度在０．２～５００ｍｇ／Ｌ范围内与峰高呈线性，检测限为０．２ｍｇ／Ｌ，加标回收率在９７．２～１０４％间，对含量为０．１ｇ／粒的氟哌酸胶囊重复测定，ＲＳＤ（ｎ＝５）为０．６７％和１．２６％．方法简便，结果准确
This paper presents a voltammetric method for the determination of norfloxacin using thin-film mercury thin film electrodes. In pH 5.6 ~ 7 acetic acid ~ sodium acetate buffer solution, norfloxacin at -1500mv has a sensitive derivative of the cathode wave for the determination of norfloxacin capsules, the results were satisfactory. The concentration of norfloxacin in the range of 0.2 ~ 500mg / L was linear with the peak height, the detection limit was 0.2mg / L, the recoveries were 97.2 ~ 104%, and the content was 0.1g / Of norfloxacin capsules with RSD (n = 5) of 0.67% and 1.26%. The method is simple and the result is accurate