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Two coordinate reactions, NdCl3·6H2O(s)+3CCl3COOH(s)(or TCA)=Nd (TCA)3·3H2O(s)+3HCl(g)+3H2O(1) and Nd(TCA)3·3H2O(s) +2C9H7NO(s)= Nd(TCA)(C9H6NO)2(s)+2CCl3COOH(s)+3H2O(1), were studied by the classical solution calorimetry at 298.15K. The mo