【摘 要】
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One kind of built,in silica adsorbent, which has high adsorption selectivity to rutin, was synthesized using molecular imprinting technology by the following st
【机 构】
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School of Chemical Engineering and Technology, TianjinUniversity, Tianjin300072, P. R. China
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One kind of built,in silica adsorbent, which has high adsorption selectivity to rutin, was synthesized using molecular imprinting technology by the following steps:synthesis of precursor from the reaction between water soluble rutin (as template molecule) and the functional monomer chloropropyltriethoxysilane, co,hydrolysis of the precursor and tetraethoxysilane (TEOS), sol,gel aging process, and removal of template molecules. The results of adsorption experiment show that this adsorbent has a high adsorption capacity for rutin, and good adsorptionselectivity towards rutin even under the interference of a flavone with a similar structure. TEM photos suggest that nanocaves corresponding to rutin were formed inside the adsorbent while FTIR spectra indicate that new bond was generated during the recognition process.
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