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利用(NH4)2S2O8在碱性溶液中与纳米PbCO3进行氧化反应,首次在较低温度下成功制备了纯相的α-PbO2纳米棒,并利用X射线衍射、扫描电镜和透射电镜对其晶型及表面形貌进行了表征。
The pure phase α-PbO2 nanorods were successfully prepared at low temperature for the first time by the oxidation reaction of (NH4) 2S2O8 with PbCO3 in alkaline solution. The XRD, SEM and TEM were used to analyze the crystal structure And surface morphology were characterized.