本文报道了全戊基取代的β-环糊精衍生物手性固定相合成和超动态法快速制备手性毛细管柱的方法,并对几种卤代烃、酯对映体进行了分离。 In this paper, the synthesis of per-pentyl-substituted β-cyclodextrin derivatives by chiral stationary phase and the ultra-dynamic method for the rapid preparation of chiral capillary columns were studied. Several enantiomers of halogenated hydrocarbons and esters were separated.