A comparative study of rhenium coatings prepared on graphite wafers by chemical vapor deposition and

来源 :稀有金属(英文版) | 被引量 : 0次 | 上传用户:simon20088
下载到本地 , 更方便阅读
声明 : 本文档内容版权归属内容提供方 , 如果您对本文有版权争议 , 可与客服联系进行内容授权或下架
论文部分内容阅读
The purity,preferred orientation,microstructure,microhardness,bonding strength,thickness uniformity and thermal stability of rhenium(Re)coatings prepared on graphite wafers by chemical vapor deposition(CVD)and electrodeposition(ED)in molten salts were comparatively studied in this paper.It was found that carbon(0.0140 wt%)and oxygen(0.0067 wt%)were the primary impuri-ties for CVD and ED Re coatings,respectively.The dif-fusion of carbon into CVD Re coating caused higher microhardness near the substrate and helped to improve the bonding strength at the same time.The preferred orienta-tion,microstructure and microhardness of ED Re coating were all susceptible to oxygen.The coating deposition uniformity of ED Re is obviously better than that of CVD Re coating,due to its intrinsic characteristics.The(002)-oriented,coarse columnar CVD Re coating exhibited better thermal stability compared with that of the(110)-oriented,fiber-like columnar ED Re coating,while the ED Re grains grew remarkably and the microstructure evolved toward the similar structure of CVD Re after annealing treatment.The diversity of Re coatings in microstructure could be attributed to the mobility of grain boundaries(affected by temperature and impurity)during deposition processes.
其他文献
弹卡式预制混凝土方桩是一种新型连接方式的混凝土预制桩,相关研究文献较少,如何通过检测确定新型基桩的沉桩质量十分重要.本文通过工程实例,证明在低应变检测弹卡桩桩身完整
该文针对三维海流观测困难及流场资料欠缺等问题,基于Argo温度和盐度观测资料,运用等密度面P矢量方法,对太平洋海区的三维流场进行了估算。该方法有效克服了常规直角坐标无法
农村公路是农业和农村发展的先导性、基础性设施,更是乡村振兴的基础之一.本文以山东典型农业大县——金乡为例,在传统节点重要度法基础上提出了基于特色产业、农业产业园重
矮塔斜拉桥宽箱梁施工常采用挂篮悬臂浇筑,在0#块施工时需要进行临时固结,因此为确保挂篮施工安全,临时固结体系必须进行结构设计验算.目前,临时固结体系一般采用两种形式:一
The purpose of this investigation was to evaluate the microstructure,high-temperature oxidation behaviour,and hardness of a seal coating under controlled exposu
运梁车载预制箱梁通过钢桁梁时,为确保钢桁梁桥安全可靠,需要对其进行监测监控.本文以跨西宝客专特大桥132 m钢桁梁为例,在钢桁梁桥梁体布设应力及挠度监测点,通过建立有限元
Sc-based nanomaterials have attracted consid-erable attention due to their unique optical properties dif-ferent from those of Ln/Y-based nanomaterials.However,s
鸡西矿业集团公司张辰煤矿西三采区3
期刊
为探究斜拉桥钢混结合段箱型格室受力性能,本文以某大跨径斜拉桥为研究对象,建立其钢混结合段箱型格室实体-壳混合有限元模型,对恒载+活载最不利工况及体系整体升降温两种荷
A multilayer(Ti/Pt/Cr/Au)resistive temperature sensor was proposed and investigated to precisely measure the temperature characteristic in microfluidic devices.