铂与钯存在于相应矿物和电解过程的阳极泥中，含量极低、分离困难。本文报导应用光化学法从阳极泥中分离铂与钯，并在一定介质条件下用光度法作了测定。结果为钯６．９６，铂４．３２ｇ／ｔ，效果满意。该法与传统化学分离法比较，工艺简便，不污染环境，分离效果好。这一开创性研究，很值得继续深入开展工作。作为铂族金属异常省的云南，开展这一研究就显得更有意义 Platinum and palladium are present in the anode slimes of the corresponding minerals and electrolytes at very low levels and are difficult to separate. This paper reports the separation of platinum and palladium from the anode slime by photochemical method and the determination of its photometric method under certain medium conditions. Results for the palladium 6.96, platinum 4.32g / t, the effect is satisfactory. The method compared with the traditional chemical separation method, the process is simple, does not pollute the environment, the separation effect is good. This groundbreaking study is worth further work. As Yunnan Province, an exceptionally prosperous PGM, it makes more sense to carry out this research