【摘 要】
：
A new environmental friendly catalyst, H4SiW12O40/PAn was prepared and identified by means of FT-IR, XRD and TG/DTA. Cyclohexanone 1,2-propanediol ketal was syn
【机 构】
：
Department of Chemistry and Environmental Engineering,College of Chemistry and Molecular Sciences
【基金项目】
：
Natural Science Foundation of Hubei Province Education Commitiee;国家自然科学基金
论文部分内容阅读
A new environmental friendly catalyst, H4SiW12O40/PAn was prepared and identified by means of FT-IR, XRD and TG/DTA. Cyclohexanone 1,2-propanediol ketal was synthesized from cyclohexanone and 1,2-propanediol in the presence of H4SiW12O40/PAn. The factors influencing the synthesis were discussed and the best conditions were found out. The optimum conditions are: molar ratio of cyclohexanone to 1,2-propanediol is 1:1.4, the quantity of catalyst is equal to 1.0%of feed stocks, and the reaction time is 40 min. H4SiW12O40/PAn is an excellent catalyst for synthesizing cyclohexanone 1,2-propanediol ketal and its yield can reach over 96.5%.
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