合成了7个未见报道的2-酰胺基-6-芳偶氮基-1,3-二氮杂艹奥化合物.用1H-NMR和元素分析确定了它们的结构.并用差示扫描量热法研究了目标化合物的热力学性质. Seven unreported 2-carboxamido-6-arylazo-1,3-diazepine compounds were synthesized and their structures were confirmed by1H-NMR and elemental analysis, and were characterized by differential scanning calorimetry Method to study the thermodynamic properties of the target compounds.