本文提出一种能快速灵敏地检测地面水和污水中苯胺类化合物的试剂盒。该方法是以 N-氯代丁二酰亚胺氧化苯胺 ,在 p H9- 1 1的碱性介质中 〔1〕,以 1 -萘酚偶联显色。显色反应所得的蓝色化合物的最大吸收波长为 61 0 nm,在苯胺浓度为 0 .2～ 8mg/L的浓度范围内符合比尔定律 ,最低检出限为 0 .0 2 mg/L ,测定的重现性在± 5 %以内。该试剂盒用于合成水样和环境水样的分析 ,回收率在 94.9～ 98.2之间。这种试剂盒可以成功地用于合成水样和环境水样的分析 This paper presents a rapid and sensitive detection of surface water and sewage aniline compounds kit. The method is N-chlorosuccinimide oxidation of aniline, pH9-1 1 in an alkaline medium 〔1〕, 1 - naphthol coupling color. The maximum absorption wavelength of the blue compound obtained from the color reaction was 61 0 nm. The Beer’s law was obeyed at a concentration range of 0.2-8 mg / L for aniline, the minimum detection limit was 0.2 mg / L, The reproducibility is within ± 5%. The kit for the synthesis of water samples and environmental water analysis, the recovery rate of 94.9 ~ 98.2 between. This kit can be successfully used in both synthetic and environmental water samples